| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
Chromatogram |
| GC: crude product | |
| column | 5CB Low Blend/MS, L=30 m, d=0.32 mm, película=0.25 µm |
| inlet | injector: 210°C, inyección partida, 1 µL |
| carrier gas | H2, presión previa de la columna 50 kPa |
| oven | 60°C (2 min), 10°C/min --> 240°C (50 min) |
| detector | FID, 310°C |
| integration | percent concentration calculated from relative peak area |
| GC: pure product | |
| column | 5CB Low Blend/MS, L=30 m, d=0.32 mm, película=0.25 µm |
| inlet | injector: 210°C, inyección partida, 1 µL |
| carrier gas | H2, presión previa de la columna 50 kPa |
| oven | 60°C (2 min), 10°C/min --> 240°C (50 min) |
| detector | FID, 310°C |
| integration | percent concentration calculated from relative peak area |