| Introduzione |
| Istruzioni |
| Schema operativo |
| Sostanze |
| Attrezzatura |
| Valutazione |
| Caratterizzazione |
| - Cromatogramma |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Reazioni secondarie |
1H-NMR |
| 1H-NMR: prodotto grezzo | |||
| 500 MHz, CDCl3 | |||
| delta [ppm] | mult. | atomi | Assegnazione |
| 1.20-1.36 | m | 3 H | 3-H, 4-H, 5-H, 6-H |
| 1.56-1.65 | m | 3 H | 3-H, 4-H, 5-H, 6-H |
| 2.04-2.10 | m | 1 H | 3-H, 4-H, 5-H, 6-H |
| 2.16-2.22 | m | 1 H | 3-H, 4-H, 5-H, 6-H |
| 2.55 | s | 1 H | O-H |
| 3.45-3.56 | m | 1 H | 1-H (-CH-OH) |
| 3.66-3.72 | m | 1 H | 2-H (-CH-Cl) |
| 7.26 | CHCl3 | ||
| 1H-NMR: trans-2-Clorocicloesanolo | |||
| 500 MHz, CDCl3 | |||
| delta [ppm] | mult. | atomi | Assegnazione |
| 1.20-1.36 | m | 3 H | 3-H, 4-H, 5-H, 6-H |
| 1.56-1.65 | m | 3 H | 3-H, 4-H, 5-H, 6-H |
| 2.04-2.10 | m | 1 H | 3-H, 4-H, 5-H, 6-H |
| 2.16-2.22 | m | 1 H | 3-H, 4-H, 5-H, 6-H |
| 2.55 | s | 1 H | O-H |
| 3.45-3.56 | m | 1 H | 1-H (-CH-OH) |
| 3.66-3.72 | m | 1 H | 2-H (-CH-Cl) |
| 7.26 | CHCl3 | ||